A facile and effective synthesis of 4-imino-3-(arylidene)- azetidine-2-thiones via phosphorus pentasulfide

作者:Amiri Ouafa; Rakib El Mostapha*; Abdelouahid Medaghri Alaoui; Faustino Maria A F; Neves Maria G P M S; Cavaleiro Jose A S
来源:Journal of Sulfur Chemistry, 2015, 36(1): 9-15.
DOI:10.1080/17415993.2014.956213

摘要

A new and an efficient synthesis of 4-imino-3-(arylidene)-azetidine-2-thiones is reported. The reaction of arylidenemalononitriles with phosphorus pentasulfide and ethanol affords the title products in good yields. Elemental analysis, infrared, H-1 NMR, C-13 NMR and mass spectral data elucidated structure of newly synthesized compounds.

  • 出版日期2015-1-2