Demineralization Effects of Hydrogen Heroxide on Bovine Enamel and Relation to Shear Bond Strength of Brackets

作者:Gonzalez Lopez Santiago*; de Medeiros Carmen Lucia Soares G; Defren Camejo Aguilar; Victoria Bolanos Carmona Maria; Sanchez Sanchez Purificacion; Menendez Nunez Mario
来源:Journal of Adhesive Dentistry, 2009, 11(6): 461-467.
DOI:10.3290/j.jad.a17651

摘要

Purpose: To measure the demineralization capacity of 37% phosphoric acid and shear bond strength (SBS) of brackets attached on bovine enamel at different times after bleaching with 30% hydrogen peroxide.
Materials and Methods: Four equally-sized pieces of each crown from 18 bovine incisors were randomly distributed among 7 groups (n = 10). After bleaching with 30% hydrogen peroxide for 1 h, specimens were stored in artificial saliva for 0 h, 24 h, or 1, 2, 3, or 4 weeks before bonding specimens to brackets. An unbleached group of specimens served as controls. Shear bond strength (SBS in MPa) was measured with a universal testing machine. Adhesive Remnant Index (ARI) scores were determined after failure of bracket bonds. To measure demineralized Ca(2+), four 4 x 4 mm sections from each of 15 bovine incisors were randomly distributed among 4 groups (n = 15). Specimens were stored in artificial saliva for 0 h, 24 h or 7 days after bleaching and then immersed in 37% phosphoric acid solution. After 15 s, 30 s, and 60 s, 5-ml aliquots of solution were removed for spectro photometry. Unbleached specimens served as controls.
Results: Larger amounts of Ca(2+) were extracted from the enamel by phosphoric acid up to 24 h after application of hydrogen peroxide, when there was also a significant decrease in bracket-enamel SBS. After 1 week, there were no changes in amounts of Ca(2+) extracted, and SBS values returned towards unbleached values.
Conclusion: Lower bracket-enamel SBS values at 24 h after bleaching are closely correlated with the larger amounts of Ca(2+) extracted from the enamel.

  • 出版日期2009