A solvothermal route to wurtzite ZnSe nanoparticles

作者:Zhan JH; Yang XG; Zhang WX; Wang DW; Xie Y; Qian YT*
来源:Journal of Materials Research, 2000, 15(3): 629-632.
DOI:10.1557/JMR.2000.0093

摘要

Zinc powder reacts with equivalent elemental selenium in solvent ethylenediamine at 120 degrees C for 6 h to form a complex, which is converted to ZnSe nanoparticles by pyrolysis or protonization. X-ray diffraction results suggest that the as-formed products have wurtzite structure. Transmission electron microscopy observation show that particles with spherical and laminar morphology were produced by pyrolysis and protonization, respectively. The formation of ZnSe nanoparticles is also investigated by infrared and thermal analysis.