A statistical prediction of density and hardness of biodegradable mechanically alloyed Mg-Zn alloy using fractional factorial design

作者：Salleh Emee Marina; Zuhailawati Hussain^*; Ramakrishnan Sivakumar; Gepreel Mohamed Abdel Hady

来源：Journal of Alloys and Compounds, 2015, 644: 476-484.

DOI：10.1016/j.jallcom.2015.04.090

• Mg-Zn alloys
• Mechanical alloying
• Hardness
• Density
• Fractional factorial design

This work aims to develop a statistical model that could be used to predict density and hardness properties of biodegradable mechanically alloyed magnesium-zinc alloy since both properties relies on densification of the powder during compaction and sintering. The effect of mechanical alloying parameters (i.e., milling time, milling speed, ball-to-powder weight ratio and percentage of zinc) and their interactions were investigated involving 4 numerical factors with 2 replicates, thus 16-run of two-level fractional factorial design. Results of analysis of variance (ANOVA), regression analysis and R-squared test indicated the good accuracy of the model. Density of sintered Mg-Zn alloy was between 1.80 and 1.99 g/cm(3) which closed to density of human bone. Hardness of pure Mg increased from 27 HV to 54 HV to 94 HV with the addition of 3-10 wt% Zn.

• 出版日期2015-9-25