Size-controlled MoO3 nanoslabs synthesized by microwave plasma-enhanced chemical vapor deposition

作者:Chang Kong Pin*; Chen Uei Shin; Shih Han C
来源:Electrochemical and Solid-State Letters, 2007, 10(3): H111-H113.
DOI:10.1149/1.2430566

摘要

In this paper, a description of a process for synthesizing MoO3 nanoslabs without using any catalyst is given. The size of the MoO3 nanostructures varying with time are clearly resolved. Time-dependent relationships vs the thickness and width of the as-grown MoO3 nanoslabs are demonstrated. Both X-ray diffraction pattern and transmission electron microscopy images indicated that MoO3 nanoslabs belong to the orthorhombic structure. Three different molybdenum-oxide bondings are differentiated by the Raman spectroscopy. Cathodoluminescene showed a significant red-orange peak based on the band structure of the MoO3.