A novel simple strategy for in situ deposition of apatite layer on AZ31B magnesium alloy for bone tissue regeneration

作者：Mousa Hamouda M; Lee Do Hee; Park Chan Hee^*; Kim Cheol Sang

来源：Applied Surface Science, 2015, 351: 55-65.

DOI：10.1016/j.apsusc.2015.05.099

• Magnesium alloys
• Simulated body fluid
• Anodizing
• Corrosion
• Biomimetic

In this study, for the first time, the degradation performance of AZ31B Mg alloy was tuned by an in situ deposition of apatite thin layer within a short time in one step. Using Taguchi method for experimental design, anodization process was designed under control conditions (time and voltage), and simulated body fluid (SBF) was used as the electrolyte to nucleate apatite-like compounds. The coated alloy was characterized through field emission scanning electron microscopy (FE-SEM), EDS, X-ray diffraction and XPS analysis. The results show that the applied voltage has a significant effect on the formation of apatite-like layers. Compared to the uncoated samples, microhardness and surface roughness of the coated samples showed remarkably different values. The potentiodynamic polarization results demonstrate that the polarization resistance of the anodized samples is higher than the substrate polarization resistance, thus improving the alloy corrosion resistant. Based on the experimental results, the proposed nanostructure apatite-like coating can offer a promising way to improve the biocompatibility and degradability properties of the Mg alloy for bone tissue regeneration.

• 出版日期2015-10-1