A facile one-pot solvothermal method for synthesis of magnetically recoverable Pd-Fe3O4 hybrid nanocatalysts for the Mizoroki-Heck reaction

作者：Zhen, Fangchen; Ran, Maofei; Chu, Wei; Jiang, Chengfa^*; Sun, Wenjing^*

来源：Chemical Physics Letters, 2018, 695: 183-189.

DOI：10.1016/j.cplett.2018.02.007

• Hybrid nanostructures
• Nanocatalyst
• One-pot method
• Pd-Fe3O4

Pd-Fe3O4 hybrid nanostructures were prepared using a simple one-pot hydrothermal method. The prepared materials were characterized by Fourier transform-infrared spectroscopy, X-ray diffraction, X-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy, inductively coupled plasma, N-2 adsorption-desorption, and vibrating sample magnetometry. This self-assembled nanosystem acted as an efficient magnetically recyclable noble metal-based multifunctional nanocatalyst. It showed excellent catalytic activity and stability for the Heck reaction of iodobenzene and styrene under mild conditions. The methods used to prepare the Pd-Fe3O4 catalysts were simple and low-cost, which will be useful for the large-scale development and application of a magnetically recoverable Pd catalyst.

• 出版日期2018-3
• 单位四川大学; 西南民族大学; 广东医科大学