2,6-Diphenyl-4-(2-thienyl)-1,4-dihydropyridine-3,5-dicarbonitrile

作者:Zhu Xiao Tong*; Zhang Ge; Ma Ning
来源:Acta Crystallographica Section E-Structure Reports Online, 2009, 65(9): O2246-U2847.
DOI:10.1107/S1600536809033339

摘要

The asymmetric unit of the title compound, C23H15N3S, contains two crystallographically independent molecules. The pyridine rings adopt envelope conformations. The thiophene rings are oriented at dihedral angles of 77.97 (4)/53.53 (4) and 78.44 (4)/57.11 (4)degrees with respect to the phenyl rings, while the dihedral angles between the phenyl rings are 48.51 (4) and 44.49 (4)degrees. In the crystal structure, intermolecular N-H center dot center dot center dot N hydrogen bonds link the molecules into chains along the c axis. The S, C and H atoms of one of the thiophene rings are disordered over two orientations, with occupancy ratios of 0.314 (15): 0.686 (15).

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