(Z)-1-Phenyl-3-(3-pyridylmethylamino)but-2-en-1-one

作者：Shi Yao Cheng^*; Zhu Bei Bei; Zhang Su Hua

来源：Acta Crystallographica Section E-Structure Reports Online, 2010, 66: O2854-U522.

DOI：10.1107/S1600536810041127

The reaction of 3-C(5)H(4)NCH(2)NH(2) and C(6)H(5)COCH(2)COCH(3) affords the title compound, C(16)H(16)N(2)O. The O = C-C = C-N portion is essentially planar [maximum deviation = 0.046 (2) angstrom] and is aligned at dihedral angles of 22.6 (1) and 78.9 (1)degrees to the phenyl and pyridyl rings, respectively. The N-H and O = C groups are linked by an intramolecular hydrogen bond. In the crystal, C-H center dot center dot center dot O hydrogen bonds and C-H center dot center dot center dot pi interactions occur.

• 出版日期2010-11
• 单位扬州大学