Mullite fiber sealing pad with favorable high-temperature rebound resilience fabricated through colloidal processing

作者:Shen, Sibo; Zhao, Yingna; Du, Haiyan; Wang, Mingchao; Zhao, Lan; Tian, Geng; Liu, Jiachen*
来源:Ceramics International, 2014, 40(6): 8905-8909.
DOI:10.1016/j.ceramint.2014.01.033

摘要

Mullite fiber sealing pad composed of chopped fibers and aqueous silica binder, having near-isotropic structure, was fabricated by a combination of vacuum filtration and colloidal processing. The fibers were randomly distributed, overlapping and interlocking to produce the matrix and pure SiO2 binder composed of a glass-ceramic structure firmly bonded fiber laps. A microwave micro-zone heater was adopted to simulate transient aerodynamic heating process and 8-cycle loading unloading test was conducted at 800 degrees C. The samples were sintered at 1300 degrees C with different silica sol concentrations (10.3-20.9 wt%). Mullite fiber pads exhibited high rebound resilience (80.9-87.6%), high compression (24-18%) and moderate Young's modulus (0.97-3.24 MPa), making it to be a promising high-temperature seal material.