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摘要
Graphene nanosheets (GNSs) were prepared using oxidation of graphite powder followed by rapid thermal exfoliation under a nitrogen atmosphere. The as-prepared samples were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), Raman spectroscopy, and Fourier transform infrared (FT-IR) spectroscopy. The specific surface area was determined using the nitrogen adsorption and desorption method. These analytic techniques revealed that the samples possessed a curled morphology consisting of a thin paper-like structure, which was made of a few graphite layers (approximately four layers) and a large specific surface area (628.5 m(2)-g(-1)). The effects of pH, adsorption time, temperature and initial concentration of RD' and Cd2+ on adsorption onto the GNSs were investigated. The maximum adsorption capacities of GNSs for Pb2+ and Cd2+ ions were approximately 460.20 and 72.39 mg.g(-1), respectively. These results indicate that the resulting high-quality GNSs can be used as an attractive adsorptive material for removing Pb2+ and Cd2+ from water.
- 出版日期2016-4-15
- 单位华南理工大学
