A high-pressure and controlled-flow gas system for catalysis research

作者:Martis Vladimir; Beale Andrew M; Detollenaere Dirk; Banerjee Dipanjan; Moroni Martine; Gosselin Fabrice; Bras Wim*
来源:JOURNAL OF SYNCHROTRON RADIATION, 2014, 21(2): 462-463.
DOI:10.1107/S1600577513031937

摘要

A high-pressure gas rig for in situ catalytic reactions at X-ray absorption spectroscopy beamline (BM26A) has been developed. The rig enables catalysts to be studied in a variety of cells under well controlled and industrially relevant operation conditions. A large variety of gas mixtures can be generated and pressures of up to 50 bar with dry gas and 20 bar with wet gas (steam) can be obtained. Analyses of reaction products can be performed using an on-line mass spectrometer.

  • 出版日期2014-3