Preparation, characterization, and catalysis application of nano-rods zinc oxide in the synthesis of 3-indolyl-3-hydroxy oxindoles in water

作者：Hosseini Sarvari Mona^*; Tavakolian Mina

来源：Applied Catalysis A: General , 2012, 441: 65-71.

DOI：10.1016/j.apcata.2012.07.009

• Nano-rods ZnO
• 3-Indolyl-3-hydroxy oxindole
• Isatin
• Indole
• Water
• Friedel-Crafts reaction

ZnO nano-rods is synthesized successfully by a new method employing Zn(OAc)(2)center dot 2H(2)O. NH3 and polyethylene glycol (PEG, M-w = 2000). X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and BET surface area measurement were used to characterize the structure and morphology of the catalyst. Nano-rods ZnO has been found highly effective and recyclable catalyst for synthesis of 3-indolyl-3-hydroxy oxindole derivatives by Friedel-Crafts reaction of indole with isatins in excellent yields, in water.

• 出版日期2012-10-28