A high yielding, one-pot synthesis of O,S-dialkyl dithiocarbonates from alcohols using Mitsunobu's reagent

作者：Chaturvedi Devdutt^*; Ray Suprabhat

来源：Tetrahedron Letters, 2007, 48(1): 149-151.

DOI：10.1016/j.tetlet.2006.10.149

• Mitsunobu's reagent
• carbon disulfide
• alcohols
• dithiocarbonates
• thiocarbarnation

A novel Mitsunobu-based protocol has been developed for the synthesis of O,S-dialkyl dithiocarbonates from a variety of primary, secondary and tertiary alcohols using carbon disulfide, in good to excellent yields. This protocol is mild and efficient compared to other reported methods.

• 出版日期2007-1-1