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摘要
A new imidooxonitridophosphate AlP(6)O(3)x(NH)(3-3x)N-9 with x approximate to 0.33 was synthesized under high-pressure high-temperature conditions. The crystal structure determination of the microcrystalline product involved a combination of electron microscopy, synchrotron X-ray diffraction and solid-state NMR. In the solid there are discrete AlN6 octahedra that interconnect imidophosphate layers. The network topology is unprecedented but is related to other nitride structures.
- 出版日期2017-3-4
