Determination of Polycyclic Aromatic Hydrocarbons in Seafood

作者：Taylor C M; Raines J M; Rodriguez J M^*

来源：Food Analytical Methods, 2013, 6(5): 1330-1336.

DOI：10.1007/s12161-012-9547-7

• Comprehensive two-dimensional gas chromatography-quadrupole mass spectrometry (GCXGC-MS)
• Polycyclic aromatic hydrocarbons (PAHs)
• Selective ion monitoring (SIM)
• Seafood
• High-pressure liquid chromatography fluorescence detector (HPLC-FL)
• Bland-Altman analysis

The aim of this project is to determine polycyclic aromatic hydrocarbons (PAHs) in several seafood matrices, i.e., fish, and mussel, by the use of comprehensive two-dimensional gas chromatography-quadrupole mass spectrometry (GCXGC-MS). The procedure involves a simple extraction of PAHs, a filtration and concentration step followed by GCXGC-MS analysis. PAHs were determined in fish tissue samples by GCXGC-MS and by a standard high-pressure liquid chromatography fluorescence detector method. A Bland-Altman analysis of the two methods was performed. It indicated equivalence between the two methods. Analysis of mussel tissue (National Institute of Standards and Technology (NIST)-SRM 2974a) was performed. The results were in line with the official results of NIST.

• 出版日期2013-10