N '-( 2-Hydroxy-3,5-diiodobenzylidene)-2-methoxybenzohydrazide

作者:Peng, San Jun*; Zhang, Fen
来源:Acta Crystallographica Section E-Structure Reports Online, 2009, 65(6): O1410-U3029.
DOI:10.1107/S160053680901914X

摘要

The title compound, C(15)H(12)I(2)N(2)O(3), was synthesized by the condensation of equimolar amounts of 3,5-diiodosalicylaldehyde and 2-methoxybenzohydrazide in a methanol solution. There are two independent molecules, A and B, in the asymmetric unit. The dihedral angle between the two benzene rings is 30.2 (2)degrees for molecule A and 21.7 (2)degrees for molecule B. There are intramolecular O-H center dot center dot center dot N and N-H center dot center dot center dot O hydrogen bonds in each molecule. The crystal studied was an inversion twin with a 0.59 (3): 0.41 (3) domain ratio.

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