摘要

A new combined method is developed for determining trace platinum, palladium, and gold in natural materials of complex composition. The method involves sorption preconcentration with solid-phase extractants obtained by impregnating polymer supports (hypercrosslinked and highly crosslinked polystyrene resins) with an imidazolium ionic liquid (1-hexadecyl-3-methylimidazolium bromide), elution with acetone under normal conditions or with a solution of thiourea in 1 M HCl under microwave heating, and the ETAAS determination of analytes in the eluate. The efficiency of the method is confirmed by the analysis of various ores and rocks.

  • 出版日期2012-6