摘要

The first in situ diffraction study of the long-known solid-state rearrangement of p-bromo-benzeneazotribenzoylmethane is reported. This proof-of-principle study demonstrates how modem laboratory X-ray powder diffraction, accompanied by up-to-date processing tools, can be used to monitor and describe mechanisms of organic solid-state reactions while it also underpins its necessity for structural characterisation of in situ formed crystalline phases.

  • 出版日期2013-7